Read 2006051009244840048.pdf text version

Agilent 1100HPLC

Agilent 1100 -

(G1322A/G1379A)

Agilent 1100

G1322A

12ml5ml/min 6min

G1379A).

1ml2ml/min 5min 5ml/min

Agilent 1100

() . (THF) (EDTA) 2-

Agilent 1100 ,

(pH 4 7) 0.00010.001 M

Agilent 1100 ,

30cm

35

Agilent 1100

1.

Purge2ml/min

2.

,

Agilent 1100 (G1311A)

Agilent 1100

Agilent 1100

Agilent 1100 (Pump Head)

Pump head screws

Agilent 1100 (Pump Head)

5

Holding/Lock Screw (PEEK)

2

3 4 6

1

7

Agilent 1100 (Pump Head)

new style

Cartridge 8

7

old style

3 4 5

Purge Valve

1

2

Outlet Ball Valve

6

Active Inlet Valve

(common to all except 1050)

Agilent 1100

Agilent 1100Seal Wash ( )

Washer

Seal

Support assembly

seal

>0.01M Agilent 1100 10%

Seal Wash

3 2

}

1

Agilent /

Agilent /

Agilent 1100

MCGV A / B D-A - Agilent 1100

MCGV () MCGV 30ml 10ml , 5ml/min 10bar, 0.2 ml/min 1/16 0.1

Agilent 1100

10 20/ 10 10

1.( 010018

47 2. 50222159 3. 2ml/min 10 4. 350bar 15 5. 5063658909051420 200bar,

Agilent /

1.

2.,

3.

3

Agilent 1100

Question?

1. A Purge 5ml/min BCD 2.Purge Purge5ml/min 10bar 3.

Agilent 1100 (G1313A)

Agilent 1100

Agilent 1100

Agilent 1100

Agilent 1100

¡°¡±, NEEDLE WASH [] 1 DRAW 5L5L 2 NEEDLE WASH vial 77 3 INJECT

2 L BYPASS 2 L 2 L Agilent 1100 200 L/min ( 10-1000 L/min) 200 L/min"DRAW" 200 L/min (10-1000 L/min) "EJECT"

VespelTM Vespel Vespel pH 2.3 9.5 Vespel pH 2.3 9.5 Vespel TefzelTM pH 2.3 9.5 Vespel Tefzel Tefzel Vespel pH Tefzel Tefzel Vespel pH Tefzel

Agilent 1100

1 2

2 2

Agilent 1100

·

·

·-

Agilent 1100

1. 2. 1 1

Agilent 1100 G1328A,G1328B)

Agilent 1100

2

1 5~6 Vespel 2 0.028 2 Agilent 1100 1 2 A. Inject ( . B.

3

3 1 2

Agilent 1100

1 2

0.2ml/min ( , 3ul). 3

Agilent 1100 (G1315B)

Agilent 1100

1024 190 --950 nm < 1 nm

190nm 800 nm VIS 470---950 nm

Agilent 1100

8 6 mm 10 mm 10 % 70 % 5L 13 L 8 1/3

3

8

4 nm 30 nm 2.5 4-nm 75 % 2

9

6 1/3 <5 % 5 % <5 % 1.4 2 2 20 % 1.4

Agilent 1100 DAD OFF

(DAM) UV UV UV- 25 s UV UV UV MWM UV UV DAM MWM Agilent 1100 DAD 656.1 nm (486 nm) 1nm

UV 1nm

190--950 nm 1 nm

Agilent

190 --- 950 nm)

1 nm Agilent 0.5- 0.7

( )

6 7 1 2 3 4 5 6 7 8 2 34 5 9 10 11

8

7 9 6 5 4 3 2 1

10

11

Agilent 1100 1. Agilent 1100 . Peakwidth(response time): DAD diagnosis VWD show module test intensity test start : 20 5 2 DAD . PMT GAIN: LAMP:standard economy RESPONSE TIME: 4S 5 1 30 . 2 65 1 ). 3 . 1 2 RID 5bar, RID 3 5 4 response time 4S 5 (P/N 0100-1847) 6 / RID /(THF)

1 2 1 3 Agilent 1100 HPLC 35 1 0.45um () Purge Purge 5ml/min 10bar Purge 5ml/min IPA ABuffer B: MeOH C: Water D: CH3CN A:B:D=20:30:50 C 100% 30minB 100% 30min seal wash 10%IPA 20 /

1. 2. 3. 4.

5.

5. IPA 5. 5. pH 9.5 2.3 tefzel 5. pH>9.5 6. VWD 40bar DAD 120bar MWD 120bar FLD 20bar RID 5bar RIDFLD 5.

HPLC

Swagelok

0.090 in

Waters

0.130 in

Parker

0.090 in

Rheodyne

0.170 in

Valco

0.080

Uptight

0.090 in

Troubleshooting LC Fittings, Part II.

J. W. Dolan and P. Upchurch.

LC/GC Magazine 6:788 (1988)

in

Color Red Green Blue

id 0.12 mm 0.17 mm 0.25 mm

EMF-- (EMF) EMF Agilent 1100 HPLC 1100 . (Not-ready) (Run) (Pre-run) (Error).

. VWD:DAD FLD: RID: purge RID ( remote ) 8 1 Not ready information( View Full menu) 2 shutdown Shutdown: Leak: system on 1 Leak 2 3 4 5 ( instrument more column thermostat ). 6 Lamp current UV lamp ignited failed.

1 diagnosis (viewdiagnosisEMF ). 1000 2000 . 2 3 diagnosis show module details maintenance logbook entry lamp replace, ok yes 1 5ml/min 10bar 2 1ml/min 20bar, 3 20bar, 1 1~2ml/min 2 3 4 ( )

1.LAN 2.GPIB

GPIB

(LAN) IP IP (properties)(local area connection), (properties), Internet Protocal(TCP/IP), IP 10.10.10.1 (local area connection)

1

enable Internet Protocal(TCP/IP) DHCP IP IP IP startprogramschemstationsconfiguration editor. IP startrun "command" DOS ping 10.10.10.1( 10.10.10.1 ping ),reply from .......; IP 2 GPIB startprogramschemstationsconfiguration editor. GPIB GPIB 1050 Variable Wavelength Detector 10 1050 Isocratic & Quaternary Pumps 16 1050 Multiple Wavelength Detector 17 1050 Diode Array Detector 17 1050 Autosampler 18 1040 Diode Array Detector 15 1046 Fluorescence Detector 12 1049 Electrochemical Detector 11 G1310 Isocratic Pump 22 G1311 Quaternary Pump 22 G1312 Binary Pump 22 G1313 Autosampler 28 G1314 Variable Wavelength Detector 24 G1315 Diode Array Detector 26 G1316 Column Compartment 27 G1321 Fluorescence detector 23 G1362 Refractive index detector 29 39500 Dual Channel Interface 13 1 2. GPIB IP 3. LAN Local Area Connection 4. GPIB (GPIB Interface Card) LAN Bootp server 8008203278

Information

44 pages

Report File (DMCA)

Our content is added by our users. We aim to remove reported files within 1 working day. Please use this link to notify us:

Report this file as copyright or inappropriate

175067